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  • (Thermodynamics)

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    PHYSICAL CHEMISTRY 352
    LABORATORY MANUAL
    FALL 2005
    Physical Chemistry 352 Lab Manual
    1. Bomb Calorimeter (Thermodynamics) …………………………………………………. 2. The Reduction of Cr (VI) by Glutathione (Consecutive Reaction Kinetics) …………… 3. Cyclic Voltammetry……………………………………………………………………... 4. Superconductivity ………………………………………………………………………. 5. Phase Diagram for a Three Component System ………………………………………… 6. Excited State Properties of 2-Naphthol Part I: Acidity Constant …………………………………………………………………. 7. Excited-State Properties of 2-Naphthol Part II: Deprotonation/Protonation Rate Constants ……………………………………… 8. Temperature-Dependent NMR Spectroscopy of Dimethylformamide ………………….. 9. Vapor Pressure of a Pure Liquid …………………………………………………………. 10. Infrared and Raman Spectrum of Carbon Disulfide ……………………………………. 11. Analysis of the Infrared Spectrum of HCL ……………………………………………… 4 14 21 26 54
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    Error Analysis. Linear Regression ………………………………………………………… Error Analysis. Propagation of Errors …………………………………………………….. Procedure for Using Hewlett-Packard Diode Array Spectrometer ………………………... Procedure for Using Perkin-Elmer LS-50B Luminescence Spectrometer ………………… Procedure for Using Perkin-Elmer Lambda -14 UV-VIS Spectrometer …………………. Procedure for Using Nicolet FTIR/Raman Spectrometer..................................................... Procedure for Using the pH Meter...................................................................................... Format for Laboratory Reports for Physical Chemistry...................................................... Safety Rules and Regulations............................................................................................
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